A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring
Theil H, Froehlich R, Glaser T (2009)
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64(11-12): 1633-1638.
Zeitschriftenaufsatz
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Autor*in
Theil, Hubert;
Froehlich, Roland;
Glaser, ThorstenUniBi
Einrichtung
Abstract / Bemerkung
The Newman-Kwart rearrangement of O-thiocarbamates to S-thiocarbamates is a versatile method for the conversion of phenols into thiophenols. The triple rearrangement of the O-trithiocarbamate 2,4,6-triacetyl-1,3,5-tri-(dimethylthiocarbamoyloxy)benzene (2) to the S-trithiocarbamate 2,4,6-triacetyl-1,3,5-tri-(dimethylthiocarbamoylthio)benzene (3) is performed, which is unprecendented for fully substituted benzene rings. The synthesis and characterization of the O-trithiocarbamate 2 and the S-trithiocarbamate 3 including the single-crystal X-ray structure analysis of compound 3 are presented.
Stichworte
Thiols;
Newman-Kwart Rearrangement;
Thiocarbamates
Erscheinungsjahr
2009
Zeitschriftentitel
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES
Band
64
Ausgabe
11-12
Seite(n)
1633-1638
ISSN
0932-0776
eISSN
1865-7117
Page URI
https://pub.uni-bielefeld.de/record/1588824
Zitieren
Theil H, Froehlich R, Glaser T. A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 2009;64(11-12):1633-1638.
Theil, H., Froehlich, R., & Glaser, T. (2009). A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 64(11-12), 1633-1638. https://doi.org/10.1515/znb-2009-11-1250
Theil, Hubert, Froehlich, Roland, and Glaser, Thorsten. 2009. “A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring”. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64 (11-12): 1633-1638.
Theil, H., Froehlich, R., and Glaser, T. (2009). A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64, 1633-1638.
Theil, H., Froehlich, R., & Glaser, T., 2009. A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 64(11-12), p 1633-1638.
H. Theil, R. Froehlich, and T. Glaser, “A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring”, ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, vol. 64, 2009, pp. 1633-1638.
Theil, H., Froehlich, R., Glaser, T.: A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 64, 1633-1638 (2009).
Theil, Hubert, Froehlich, Roland, and Glaser, Thorsten. “A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring”. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64.11-12 (2009): 1633-1638.
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