Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy

Mix A, Lamm J-H, Schwabedissen J, Gebel E, Stammler H-G, Mitzel NW (2022)
Chemical Communications.

Zeitschriftenaufsatz | E-Veröff. vor dem Druck | Englisch
 
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Abstract / Bemerkung
Equimolar mixtures of pyridine (Py) with para-halotetrafluoropyridine (BrTFP and ITFP) were investigated by VT-diffusion NMR experiments. The formation of a halogen-bond-stabilized ITFP·Py complex was detected upon cooling a solution in methylcyclohexane-d14 to 260 K; this allows monitoring a halogen-bond-driven aggregation process preceding crystallization in solution.
Erscheinungsjahr
2022
Zeitschriftentitel
Chemical Communications
eISSN
1364-548X
Page URI
https://pub.uni-bielefeld.de/record/2960628

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Mix A, Lamm J-H, Schwabedissen J, Gebel E, Stammler H-G, Mitzel NW. Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy. Chemical Communications. 2022.
Mix, A., Lamm, J. - H., Schwabedissen, J., Gebel, E., Stammler, H. - G., & Mitzel, N. W. (2022). Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy. Chemical Communications. https://doi.org/10.1039/d1cc05925d
Mix, A., Lamm, J. - H., Schwabedissen, J., Gebel, E., Stammler, H. - G., and Mitzel, N. W. (2022). Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy. Chemical Communications.
Mix, A., et al., 2022. Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy. Chemical Communications.
A. Mix, et al., “Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy”, Chemical Communications, 2022.
Mix, A., Lamm, J.-H., Schwabedissen, J., Gebel, E., Stammler, H.-G., Mitzel, N.W.: Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy. Chemical Communications. (2022).
Mix, Andreas, Lamm, Jan-Hendrik, Schwabedissen, Jan, Gebel, Erich, Stammler, Hans-Georg, and Mitzel, Norbert W. “Monitoring dynamic pre-crystallization aggregation processes in solution by VT-DOSY-NMR spectroscopy”. Chemical Communications (2022).

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