Biconcave and Convex-Concave Tribenzotriquinacene Dimers

Li Z-M, Li Y-W, Cao X-P, Chow H-F, Kuck D (2018)
JOURNAL OF ORGANIC CHEMISTRY 83(7): 3433-3440.

Zeitschriftenaufsatz | Veröffentlicht | Englisch
 
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Autor*in
Li, Zhi-Min; Li, Ya-Wei; Cao, Xiao-Ping; Chow, Hak-Fun; Kuck, DietmarUniBi
Abstract / Bemerkung
A new chiral tribenzotriquinacene bearing an ortho-bromoaniline nudeus was synthesized and optically resolved. The individual enantiomers, the absolute configuration of which was confirmed by single-crystal X-ray structure analysis, were stereoselectively converted into the same pyrazine-fused syn-bis-TBTQ derivative by chirality-assisted Buchwald-Hartwig amination. The corresponding diastereomeric anti-dimer was obtained alongside the syndimer from the racemic sample under similar reaction conditions. X-ray structure analysis of the dimers confirmed the mutual biconcave and convex-concave configuration of their TBTQ moieties and the preservation of the orthogonal orientation of the indane wings within each of them.
Erscheinungsjahr
2018
Zeitschriftentitel
JOURNAL OF ORGANIC CHEMISTRY
Band
83
Ausgabe
7
Seite(n)
3433-3440
ISSN
0022-3263
Page URI
https://pub.uni-bielefeld.de/record/2920274

Zitieren

Li Z-M, Li Y-W, Cao X-P, Chow H-F, Kuck D. Biconcave and Convex-Concave Tribenzotriquinacene Dimers. JOURNAL OF ORGANIC CHEMISTRY. 2018;83(7):3433-3440.
Li, Z. - M., Li, Y. - W., Cao, X. - P., Chow, H. - F., & Kuck, D. (2018). Biconcave and Convex-Concave Tribenzotriquinacene Dimers. JOURNAL OF ORGANIC CHEMISTRY, 83(7), 3433-3440. doi:10.1021/acs.joc.8b00375
Li, Z. - M., Li, Y. - W., Cao, X. - P., Chow, H. - F., and Kuck, D. (2018). Biconcave and Convex-Concave Tribenzotriquinacene Dimers. JOURNAL OF ORGANIC CHEMISTRY 83, 3433-3440.
Li, Z.-M., et al., 2018. Biconcave and Convex-Concave Tribenzotriquinacene Dimers. JOURNAL OF ORGANIC CHEMISTRY, 83(7), p 3433-3440.
Z.-M. Li, et al., “Biconcave and Convex-Concave Tribenzotriquinacene Dimers”, JOURNAL OF ORGANIC CHEMISTRY, vol. 83, 2018, pp. 3433-3440.
Li, Z.-M., Li, Y.-W., Cao, X.-P., Chow, H.-F., Kuck, D.: Biconcave and Convex-Concave Tribenzotriquinacene Dimers. JOURNAL OF ORGANIC CHEMISTRY. 83, 3433-3440 (2018).
Li, Zhi-Min, Li, Ya-Wei, Cao, Xiao-Ping, Chow, Hak-Fun, and Kuck, Dietmar. “Biconcave and Convex-Concave Tribenzotriquinacene Dimers”. JOURNAL OF ORGANIC CHEMISTRY 83.7 (2018): 3433-3440.

1 Zitation in Europe PMC

Daten bereitgestellt von Europe PubMed Central.

Stereoselective synthesis of enantiomerically pure bowl-shaped hydroxytribenzotriquinacenes.
Rommelmann P, Nachtigall B, Guntelmann T, Gröger H, Kuck D., Org Biomol Chem 16(31), 2018
PMID: 30033471

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