Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process
Rulli G, Fredriksen KA, Duangdee N, Bonge-Hansen T, Berkessel A, Gröger H (2013)
Synthesis 45(18): 2512-2519.
Zeitschriftenaufsatz
| Veröffentlicht | Englisch
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Autor*in
Rulli, Giuseppe;
Fredriksen, Kim A.;
Duangdee, Nongnaphat;
Bonge-Hansen, Tore;
Berkessel, Albrecht;
Gröger, HaraldUniBi
Abstract / Bemerkung
A detailed study on the impact of the catalyst loading on conversion and enantioselectivity of the direct aldol reaction of an aldehyde and acetone in aqueous solvent with nonimmobilized and immobilized proline amide-based organocatalysts is described. Based on a polymer-supported catalyst, batch and semi-continuously operating processes, comprising recycling studies in the latter case, were investigated.
Stichworte
enantioselectivity;
aldol reaction;
catalysis;
supported catalysis;
polymers
Erscheinungsjahr
2013
Zeitschriftentitel
Synthesis
Band
45
Ausgabe
18
Seite(n)
2512-2519
ISSN
0039-7881
eISSN
1437-210X
Page URI
https://pub.uni-bielefeld.de/record/2635953
Zitieren
Rulli G, Fredriksen KA, Duangdee N, Bonge-Hansen T, Berkessel A, Gröger H. Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process. Synthesis. 2013;45(18):2512-2519.
Rulli, G., Fredriksen, K. A., Duangdee, N., Bonge-Hansen, T., Berkessel, A., & Gröger, H. (2013). Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process. Synthesis, 45(18), 2512-2519. doi:10.1055/s-0033-1338509
Rulli, Giuseppe, Fredriksen, Kim A., Duangdee, Nongnaphat, Bonge-Hansen, Tore, Berkessel, Albrecht, and Gröger, Harald. 2013. “Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process”. Synthesis 45 (18): 2512-2519.
Rulli, G., Fredriksen, K. A., Duangdee, N., Bonge-Hansen, T., Berkessel, A., and Gröger, H. (2013). Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process. Synthesis 45, 2512-2519.
Rulli, G., et al., 2013. Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process. Synthesis, 45(18), p 2512-2519.
G. Rulli, et al., “Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process”, Synthesis, vol. 45, 2013, pp. 2512-2519.
Rulli, G., Fredriksen, K.A., Duangdee, N., Bonge-Hansen, T., Berkessel, A., Gröger, H.: Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process. Synthesis. 45, 2512-2519 (2013).
Rulli, Giuseppe, Fredriksen, Kim A., Duangdee, Nongnaphat, Bonge-Hansen, Tore, Berkessel, Albrecht, and Gröger, Harald. “Asymmetric Organocatalytic Aldol Reaction in Water: Mechanistic Insights and Development of a Semi-Continuously Operating Process”. Synthesis 45.18 (2013): 2512-2519.
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