Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals

Schaate A, Roy P, Godt A, Lippke J, Waltz F, Wiebcke M, Behrens P (2011)
Chemistry 17(24): 6643-6651.

Zeitschriftenaufsatz | Veröffentlicht | Englisch
 
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Autor*in
Schaate, Andreas; Roy, PascalUniBi; Godt, AdelheidUniBi; Lippke, Jann; Waltz, Florian; Wiebcke, Michael; Behrens, Peter
Abstract / Bemerkung
We present an investigation on the influence of benzoic acid, acetic acid, and water on the syntheses of the Zr-based metal-organic frameworks Zr-bdc (UiO-66), Zr-bdc-NH(2) (UiO-66-NH(2)), Zr-bpdc (UiO-67), and Zr-tpdc-NH(2) (UiO-68-NH(2)) (H(2)bdc: terephthalic acid, H(2)bpdc: biphenyl-4,4'-dicarboxylic acid, H(2)tpdc: terphenyl-4,4 ''-dicarboxylic acid). By varying the amount of benzoic or acetic acid, the synthesis of Zr-bdc can be modulated. With increasing concentration of the modulator, the products change from intergrown to individual crystals, the size of which can be tuned. Addition of benzoic acid also affects the size and morphology of Zr-bpdc and, additionally, makes the synthesis of Zr-bpdc highly reproducible. The control of crystal and particle size is proven by powder XRD, SEM and dynamic light scattering (DLS) measurements. Thermogravimetric analysis (TGA) and Ar sorption experiments show that the materials from modulated syntheses can be activated and that they exhibit high specific surface areas. Water proved to be essential for the formation of well-ordered Zr-bdc-NH(2). Zr-tpdc-NH(2), a material with a structure analogous to that of Zr-bdc and Zr-bpdc, but with the longer, functionalized linker 2'-amino-1,1':4', 1 ''-terphenyl-4,4 ''-dicarboxylic acid, was obtained as single crystals. This allowed the first single-crystal structural analysis of a Zr-based metal-organic framework.
Stichworte
zirconium; nanoparticles; modulation approach; metal-organic frameworks; microporous materials
Erscheinungsjahr
2011
Zeitschriftentitel
Chemistry
Band
17
Ausgabe
24
Seite(n)
6643-6651
ISSN
0947-6539
Page URI
https://pub.uni-bielefeld.de/record/2307277

Zitieren

Schaate A, Roy P, Godt A, et al. Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals. Chemistry. 2011;17(24):6643-6651.
Schaate, A., Roy, P., Godt, A., Lippke, J., Waltz, F., Wiebcke, M., & Behrens, P. (2011). Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals. Chemistry, 17(24), 6643-6651. https://doi.org/10.1002/chem.201003211
Schaate, Andreas, Roy, Pascal, Godt, Adelheid, Lippke, Jann, Waltz, Florian, Wiebcke, Michael, and Behrens, Peter. 2011. “Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals”. Chemistry 17 (24): 6643-6651.
Schaate, A., Roy, P., Godt, A., Lippke, J., Waltz, F., Wiebcke, M., and Behrens, P. (2011). Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals. Chemistry 17, 6643-6651.
Schaate, A., et al., 2011. Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals. Chemistry, 17(24), p 6643-6651.
A. Schaate, et al., “Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals”, Chemistry, vol. 17, 2011, pp. 6643-6651.
Schaate, A., Roy, P., Godt, A., Lippke, J., Waltz, F., Wiebcke, M., Behrens, P.: Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals. Chemistry. 17, 6643-6651 (2011).
Schaate, Andreas, Roy, Pascal, Godt, Adelheid, Lippke, Jann, Waltz, Florian, Wiebcke, Michael, and Behrens, Peter. “Modulated Synthesis of Zr-Based Metal-Organic Frameworks: From Nano to Single Crystals”. Chemistry 17.24 (2011): 6643-6651.

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