First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization
Agena C, Wolff C, Mattay J (2001)
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (15): 2977-2981.
Zeitschriftenaufsatz
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Autor*in
Agena, C;
Wolff, C;
Mattay, JochenUniBi
Abstract / Bemerkung
The monofunctionalization of rccc-2,8,14,20-tetramethylresorc[4]arene (1) with (S)-(+)-10-camphorsulfonyl chloride led to a diastereomeric mixture of (+)-2a and (-)-2b, which were separated by HPLC, Permethylation of these compounds was achieved with diazomethane. The inherently chiral, enantiomerically pure resorc[4]arenes (+)-4 and (-)-4 were obtained by alkaline hydrolysis of (+)-3a or (+)-3b, respectively.
Stichworte
calixarenes;
resorc[4]arenes;
macrocycles;
chirality;
asymmetric synthesis
Erscheinungsjahr
2001
Zeitschriftentitel
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Ausgabe
15
Seite(n)
2977-2981
ISSN
1434-193X
Page URI
https://pub.uni-bielefeld.de/record/1616607
Zitieren
Agena C, Wolff C, Mattay J. First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY. 2001;(15):2977-2981.
Agena, C., Wolff, C., & Mattay, J. (2001). First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY(15), 2977-2981. https://doi.org/10.1002/1099-0690(200108)2001:15<2977::AID-EJOC2977>3.0.CO;2-L
Agena, C, Wolff, C, and Mattay, Jochen. 2001. “First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization”. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, no. 15: 2977-2981.
Agena, C., Wolff, C., and Mattay, J. (2001). First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2977-2981.
Agena, C., Wolff, C., & Mattay, J., 2001. First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, (15), p 2977-2981.
C. Agena, C. Wolff, and J. Mattay, “First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization”, EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2001, pp. 2977-2981.
Agena, C., Wolff, C., Mattay, J.: First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY. 2977-2981 (2001).
Agena, C, Wolff, C, and Mattay, Jochen. “First synthesis, isolation and complete characterization of both enantiomers of inherently chiral resorc[4]arenes by monofunctionalization”. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY 15 (2001): 2977-2981.
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