Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles
Fesun IM, Rozhenko AB, Timoshenko VM (2006)
JOURNAL OF FLUORINE CHEMISTRY 127(6): 774-779.
Zeitschriftenaufsatz
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Autor*in
Fesun, Igor M.;
Rozhenko, Alexander B.;
Timoshenko, Vadim M.
Einrichtung
Abstract / Bemerkung
Treatment of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with 2 equivalents of sodium sulfide gives after acidification 3,4-difluoro-2-mercapto-1,6,6a gimel(4)-trithiapentalene, which can be further reduced by sodium sulfide to 3,5-difluoro-4-mercapto-thiopyran-2-thione. (c) 2006 Elsevier B.V. All rights reserved.
Stichworte
calculations;
thiopyranthione;
trithiapentalene;
2-dithiole-3-thione;
1;
reduction;
thiocarbonyl compounds;
DFT;
MP2
Erscheinungsjahr
2006
Zeitschriftentitel
JOURNAL OF FLUORINE CHEMISTRY
Band
127
Ausgabe
6
Seite(n)
774-779
ISSN
0022-1139
Page URI
https://pub.uni-bielefeld.de/record/1599014
Zitieren
Fesun IM, Rozhenko AB, Timoshenko VM. Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles. JOURNAL OF FLUORINE CHEMISTRY. 2006;127(6):774-779.
Fesun, I. M., Rozhenko, A. B., & Timoshenko, V. M. (2006). Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles. JOURNAL OF FLUORINE CHEMISTRY, 127(6), 774-779. https://doi.org/10.1016/j.jfluchem.2006.02.013
Fesun, Igor M., Rozhenko, Alexander B., and Timoshenko, Vadim M. 2006. “Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles”. JOURNAL OF FLUORINE CHEMISTRY 127 (6): 774-779.
Fesun, I. M., Rozhenko, A. B., and Timoshenko, V. M. (2006). Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles. JOURNAL OF FLUORINE CHEMISTRY 127, 774-779.
Fesun, I.M., Rozhenko, A.B., & Timoshenko, V.M., 2006. Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles. JOURNAL OF FLUORINE CHEMISTRY, 127(6), p 774-779.
I.M. Fesun, A.B. Rozhenko, and V.M. Timoshenko, “Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles”, JOURNAL OF FLUORINE CHEMISTRY, vol. 127, 2006, pp. 774-779.
Fesun, I.M., Rozhenko, A.B., Timoshenko, V.M.: Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles. JOURNAL OF FLUORINE CHEMISTRY. 127, 774-779 (2006).
Fesun, Igor M., Rozhenko, Alexander B., and Timoshenko, Vadim M. “Reduction of 4-fluoro-5-(1,1,2,2-tetrafluoroethyl)-3H-1,2-dithiole-3-thione with sodium sulfide: Synthesis of fluoro-containing sulfur-rich heterocycles”. JOURNAL OF FLUORINE CHEMISTRY 127.6 (2006): 774-779.
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