Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]

Weber L, Bastian H, Müller A, Bögge H (1991)
Organometallics 10(1): 2-4.

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Abstract
The diphosphenyl complex (eta-5-C5Me5)-(CO)2Fe-P = P-Mes* (Mes* = 2,4,6-tBu3C6H2) undergoes a [1 + 4] cheletropic cycloaddition with the azodicarboxylates RO2C-N = N-CO2R (R = Et, tBu) to give the metal-substituted oxadiazaphospholenes (eta-5-C5Me5) (CO)2Fe-P-Activated(= P-Mes*)[N(CO2R)N = C(OR)O] with exocyclic P = P bonds. The molecular structure of one of the compounds (R = Et) was elucidated by a single-crystal X-ray analysis.
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Weber L, Bastian H, Müller A, Bögge H. Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]. Organometallics. 1991;10(1):2-4.
Weber, L., Bastian, H., Müller, A., & Bögge, H. (1991). Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]. Organometallics, 10(1), 2-4.
Weber, L., Bastian, H., Müller, A., and Bögge, H. (1991). Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]. Organometallics 10, 2-4.
Weber, L., et al., 1991. Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]. Organometallics, 10(1), p 2-4.
L. Weber, et al., “Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]”, Organometallics, vol. 10, 1991, pp. 2-4.
Weber, L., Bastian, H., Müller, A., Bögge, H.: Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]. Organometallics. 10, 2-4 (1991).
Weber, Lothar, Bastian, Holger, Müller, Achim, and Bögge, Hartmut. “Cycloaddition reactions of the diphosphenyl complex (η5-C5Me5)(CO)2Fe-P=P-Mes* (Mes* = 2,4,6-tBu3C6H2) with Azo Dicarboxylates. X-ray Structure Analysis of (η5-C5Me5)(CO)2Fe-P(=PMes*)[N(CO2Et)-NC(OEt)O]”. Organometallics 10.1 (1991): 2-4.
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