Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene

Suenkel K, Weigand S, Hoffmann A, Blomeyer S, Reuter C, Vishnevskiy Y, Mitzel NW (2015)
Journal of the American Chemical Society 137(1): 126-129.

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Starting from ferrocene, pentafluoroferrocene [Fe(C5F5)(C5H5)] can be prepared in five steps via a one-pot lithiation-electrophilic fluorination strategy. Pentafluoroferrocene was characterized by multinuclear NMR and IR spectroscopy, by cyclovoltammetry as well as X-ray (solid) and electron diffraction (gas) and the experimental results compared with DFT calculations.
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Suenkel K, Weigand S, Hoffmann A, et al. Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene. Journal of the American Chemical Society. 2015;137(1):126-129.
Suenkel, K., Weigand, S., Hoffmann, A., Blomeyer, S., Reuter, C., Vishnevskiy, Y., & Mitzel, N. W. (2015). Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene. Journal of the American Chemical Society, 137(1), 126-129. doi:10.1021/ja511588p
Suenkel, K., Weigand, S., Hoffmann, A., Blomeyer, S., Reuter, C., Vishnevskiy, Y., and Mitzel, N. W. (2015). Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene. Journal of the American Chemical Society 137, 126-129.
Suenkel, K., et al., 2015. Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene. Journal of the American Chemical Society, 137(1), p 126-129.
K. Suenkel, et al., “Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene”, Journal of the American Chemical Society, vol. 137, 2015, pp. 126-129.
Suenkel, K., Weigand, S., Hoffmann, A., Blomeyer, S., Reuter, C., Vishnevskiy, Y., Mitzel, N.W.: Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene. Journal of the American Chemical Society. 137, 126-129 (2015).
Suenkel, Karlheinz, Weigand, Stefan, Hoffmann, Alexander, Blomeyer, Sebastian, Reuter, Christian, Vishnevskiy, Yury, and Mitzel, Norbert W. “Synthesis and Characterization of 1,2,3,4,5-Pentafluoroferrocene”. Journal of the American Chemical Society 137.1 (2015): 126-129.
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Dichlorophosphanyl isocyanate - spectroscopy, conformation and molecular structure in the gas phase and the solid state.
Li D, Schwabedissen J, Stammler HG, Mitzel NW, Willner H, Zeng X., Phys Chem Chem Phys 18(37), 2016
PMID: 27711553
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