DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS

JANSEN U, RUNSINK J, Mattay J (1991)
Liebigs Annalen der Chemie (3): 283-285.

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Abstract
The two diastereomers of spirocyclic 5,6-dimethyl-4H-1,3-dioxin-4-one (5,6) have been synthesized by acetalization of tert-butyl 2-methyl-3-oxobutanoate (2) with (-)-menthone (4). Their structures have been determined by NMR analysis.
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JANSEN U, RUNSINK J, Mattay J. DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS. Liebigs Annalen der Chemie. 1991;(3):283-285.
JANSEN, U., RUNSINK, J., & Mattay, J. (1991). DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS. Liebigs Annalen der Chemie(3), 283-285.
JANSEN, U., RUNSINK, J., and Mattay, J. (1991). DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS. Liebigs Annalen der Chemie, 283-285.
JANSEN, U., RUNSINK, J., & Mattay, J., 1991. DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS. Liebigs Annalen der Chemie, (3), p 283-285.
U. JANSEN, J. RUNSINK, and J. Mattay, “DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS”, Liebigs Annalen der Chemie, 1991, pp. 283-285.
JANSEN, U., RUNSINK, J., Mattay, J.: DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS. Liebigs Annalen der Chemie. 283-285 (1991).
JANSEN, U, RUNSINK, J, and Mattay, Jochen. “DIASTEREOMERIC 5,6-DIMETHYL-4H-1,3-DIOXIN-4-ONES FROM (-)-(1R,4S)-MENTHONE - SYNTHESIS AND NMR ANALYSIS”. Liebigs Annalen der Chemie 3 (1991): 283-285.
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