The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane

Mitzel NW, Vojinovic K (2003)
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 58(7): 708-710.

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Abstract
Single crystals of chlorodimethyl(dimethylamino)silane, Me2NSiMe2Cl, and dimethyl-bis-(dimethylamino)silane, (Me2N)(2)SiMe2, have been grown in situ from the melt at low temperatures and their structures determined by X-ray diffraction. Important structural parameters (Angstrom/degrees): Me2NSiMe2Cl (C2/m) Si-N 1.686(2), Si-C 1.851(1), Si-Cl 2.109(1), N-Si-Cl 111.7(1), C-Si-Cl 105.1(1), C-N-C 112.8(2), Si-N-C 123.4(1); (Me2N)(2)SiMe2 (P2(1)/c) Si-N(1) 1.725(1), Si-C(1) 1.868(1), N(1)-Si-N(2) 105.7(1), C(3)- N(1)-C(4) 111.6(1), Si-N(1)-C(3) 122.4(1), Si-N(1)-C(4) 120.0(1).
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Mitzel NW, Vojinovic K. The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 2003;58(7):708-710.
Mitzel, N. W., & Vojinovic, K. (2003). The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 58(7), 708-710.
Mitzel, N. W., and Vojinovic, K. (2003). The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 58, 708-710.
Mitzel, N.W., & Vojinovic, K., 2003. The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 58(7), p 708-710.
N.W. Mitzel and K. Vojinovic, “The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane”, ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, vol. 58, 2003, pp. 708-710.
Mitzel, N.W., Vojinovic, K.: The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 58, 708-710 (2003).
Mitzel, Norbert W., and Vojinovic, K. “The crystal structures of chlorodimethyl(dimethylamino)silane and dimethyl-bis-(dimethylamino)silane”. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 58.7 (2003): 708-710.
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