A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex

Siemeling U, Neumann B, Stammler H-G (1994)
Zeitschrift für Naturforschung, B: Chemical Sciences 49(5): 683-686.

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The novel cyclopentadiene HMe4C5CH2CMe2py [py = 2-(4-tert-butyl)pyridyl] 2H has been prepared from tetramethylfulvene and lithiated 2-isopropyl-4-tert-butylpyridine. Lithiation of 2H with Bu n Li and subsequent reaction with FeCl2 yields the ferrocene (2) 2Fe, which crystallizes in the triclinic space group P (1) with a = 8.368(1), b = 8.468(1), c = 14.313(1) Å, [alpha] = 80.64(1), [beta] = 86.67(1), [gamma] = 80.12(1)° and V = 985.4(2) Å (3).
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Siemeling U, Neumann B, Stammler H-G. A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex. Zeitschrift für Naturforschung, B: Chemical Sciences. 1994;49(5):683-686.
Siemeling, U., Neumann, B., & Stammler, H. - G. (1994). A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex. Zeitschrift für Naturforschung, B: Chemical Sciences, 49(5), 683-686.
Siemeling, U., Neumann, B., and Stammler, H. - G. (1994). A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex. Zeitschrift für Naturforschung, B: Chemical Sciences 49, 683-686.
Siemeling, U., Neumann, B., & Stammler, H.-G., 1994. A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex. Zeitschrift für Naturforschung, B: Chemical Sciences, 49(5), p 683-686.
U. Siemeling, B. Neumann, and H.-G. Stammler, “A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex”, Zeitschrift für Naturforschung, B: Chemical Sciences, vol. 49, 1994, pp. 683-686.
Siemeling, U., Neumann, B., Stammler, H.-G.: A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex. Zeitschrift für Naturforschung, B: Chemical Sciences. 49, 683-686 (1994).
Siemeling, Ulrich, Neumann, Beate, and Stammler, Hans-Georg. “A pentamethylcyclopentadienyl ligand functionalized with a pendant pyridyl group - crystal-structure of its ferrocene-type iron complex”. Zeitschrift für Naturforschung, B: Chemical Sciences 49.5 (1994): 683-686.
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