PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM

Müller A, Khan MI, Krickemeyer E, Bögge H (1991)
INORGANIC CHEMISTRY 30(9): 2040-2043.

Journal Article | Published | English

No fulltext has been uploaded

Abstract
(PPh4)[Ru(NO)(NH3)(S4)2] has been prepared by reacting trichloronitrosylruthenium with a solution of tetraphenylphosphonium polysulfide in ammoniacal acetonitrile and characterized by X-ray crystallography. Crystal data at 21-degrees-C: dark red-brown crystals, monoclinic space group P2(1)/n, a = 11.341 (3) angstrom, b = 13.091 (3) angstrom, c = 20.829 (5) angstrom, beta = 104.93 (2)-degrees, V = 2987.8 angstrom 3, Z = 4; the structure was refined to R = 0.046 and R(w) = 0.043 for 4986 unique reflections. Ru-N(NO), Ru-N(NH3), and Ru-S distances are 1.717 (4), 2.146 (4), and 2.394 (1)-2.408 (1) angstrom, respectively. The Ru-NO moiety is approximately linear, with an Ru-N-O angle of 175.7 (3)-degrees.
Publishing Year
ISSN
PUB-ID

Cite this

Müller A, Khan MI, Krickemeyer E, Bögge H. PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM. INORGANIC CHEMISTRY. 1991;30(9):2040-2043.
Müller, A., Khan, M. I., Krickemeyer, E., & Bögge, H. (1991). PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM. INORGANIC CHEMISTRY, 30(9), 2040-2043.
Müller, A., Khan, M. I., Krickemeyer, E., and Bögge, H. (1991). PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM. INORGANIC CHEMISTRY 30, 2040-2043.
Müller, A., et al., 1991. PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM. INORGANIC CHEMISTRY, 30(9), p 2040-2043.
A. Müller, et al., “PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM”, INORGANIC CHEMISTRY, vol. 30, 1991, pp. 2040-2043.
Müller, A., Khan, M.I., Krickemeyer, E., Bögge, H.: PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM. INORGANIC CHEMISTRY. 30, 2040-2043 (1991).
Müller, Achim, Khan, M. I., Krickemeyer, Erich, and Bögge, Hartmut. “PREPARATION AND X-RAY STRUCTURE OF TETRAPHENYLPHOSPHONIUM AMMINEBIS(TETRASULFIDO)NITROSYLRUTHENATE, (PPH4)[RU(NO)(NH3)(S4)2] - THE 1ST POLYSULFIDO NITROSYL COMPLEX OF RUTHENIUM”. INORGANIC CHEMISTRY 30.9 (1991): 2040-2043.
This data publication is cited in the following publications:
This publication cites the following data publications:

Export

0 Marked Publications

Open Data PUB

Web of Science

View record in Web of Science®

Search this title in

Google Scholar