K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur

Botar A, Botar B, Gili P, Müller A, Meyer J, Bögge H, Schmidtmann M (1996)
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE 622(9): 1435-1440.

Journal Article | Published | German

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K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthesis and structure
Abstract
K-11[HSn3II((PW9O34)-O-VI)(2)]. 27 H2O 1 can be synthesized in an ''one-pot reaction'' from commercially obtainable educts (SnCl2; Na2HPO4 . 7 H2O, Na2WO4 . 2H(2)O) in high yields and has been characterized by elemental analysis, IR/Raman-, UV/Vis-spectroscopy as well as by X-ray crystal structure analysis. The example of 1 again demonstrates the validity of our working hypothesis, that polyoxometalates can be obtained by linking highly charged, transferable building blocks by cationic centres within the scope of an optimal charge control. For structural details see ''Inhaltsubersicht''.
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Botar A, Botar B, Gili P, et al. K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE. 1996;622(9):1435-1440.
Botar, A., Botar, B., Gili, P., Müller, A., Meyer, J., Bögge, H., & Schmidtmann, M. (1996). K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 622(9), 1435-1440.
Botar, A., Botar, B., Gili, P., Müller, A., Meyer, J., Bögge, H., and Schmidtmann, M. (1996). K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE 622, 1435-1440.
Botar, A., et al., 1996. K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 622(9), p 1435-1440.
A. Botar, et al., “K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur”, ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, vol. 622, 1996, pp. 1435-1440.
Botar, A., Botar, B., Gili, P., Müller, A., Meyer, J., Bögge, H., Schmidtmann, M.: K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE. 622, 1435-1440 (1996).
Botar, Alexandru, Botar, Bogdan, Gili, Pedro, Müller, Achim, Meyer, Jochen, Bögge, Hartmut, and Schmidtmann, Marc. “K-11[HSn3II((PW9O34)-O-VI)(2)]center dot 27H(2)O - Synthese und Struktur”. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE 622.9 (1996): 1435-1440.
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