An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes

Friedrichs F, Murphy B, Nayrat D, Ahner T, Funke M, Ryan M, Lex J, Mattay J, Oelgemoeller M (2008)
SYNLETT 2008(20): 3137-3140.

Journal Article | Published | English

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Abstract
Irradiation of 1,4-naphthoquinone at 300 25 rim in benzene and in the presence of aliphatic aldehydes readily yields acylated hydroquinones in good to high yields. The developed protocol represents a significant improvement over the original procedure using medium-pressure mercury lamps. Subsequent oxidation gives the corresponding acylated quinones.
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Friedrichs F, Murphy B, Nayrat D, et al. An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes. SYNLETT. 2008;2008(20):3137-3140.
Friedrichs, F., Murphy, B., Nayrat, D., Ahner, T., Funke, M., Ryan, M., Lex, J., et al. (2008). An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes. SYNLETT, 2008(20), 3137-3140.
Friedrichs, F., Murphy, B., Nayrat, D., Ahner, T., Funke, M., Ryan, M., Lex, J., Mattay, J., and Oelgemoeller, M. (2008). An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes. SYNLETT 2008, 3137-3140.
Friedrichs, F., et al., 2008. An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes. SYNLETT, 2008(20), p 3137-3140.
F. Friedrichs, et al., “An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes”, SYNLETT, vol. 2008, 2008, pp. 3137-3140.
Friedrichs, F., Murphy, B., Nayrat, D., Ahner, T., Funke, M., Ryan, M., Lex, J., Mattay, J., Oelgemoeller, M.: An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes. SYNLETT. 2008, 3137-3140 (2008).
Friedrichs, Ferdinand, Murphy, Brian, Nayrat, Delphine, Ahner, Torsten, Funke, Mario, Ryan, Michael, Lex, Johann, Mattay, Jochen, and Oelgemoeller, Michael. “An Improved Procedure for the Photoacylation of 1,4-Naphthoquinone with Aliphatic Aldehydes”. SYNLETT 2008.20 (2008): 3137-3140.
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