Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation

Stoll I, Brodbeck R, Neumann B, Stammler H-G, Mattay J (2009)
CRYSTENGCOMM 11(2): 306-317.

Journal Article | Published | English

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Abstract
The arene functionalised 2-aminopyrimidines 4-6 have been synthesized. These compounds bear an aminopyrimidine unit for self assembly based on hydrogen bonding and an arene moiety which is suitable for solid state pi-pi-interactions. The crystal structures show networks built up by coexisting non covalent interactions. Also the hexafluorobenzene co-crystals of this series of compounds were investigated by X-ray structure determination. Herein, the arene-perfluoroarene interaction is crucial for crystal structure organisation, but still in coexistence with hydrogen bonding motives. The silver tetrafluoroborate complexes of the aminopyrimidines [Ag(L)(2)](+) BF4- (L = 4-6) were synthesized and the solid state structures determined. Here, the hydrogen bonding motive is replaced by the silver coordination and the arene-arene interaction was investigated joining the silver assembling motive.
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Stoll I, Brodbeck R, Neumann B, Stammler H-G, Mattay J. Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation. CRYSTENGCOMM. 2009;11(2):306-317.
Stoll, I., Brodbeck, R., Neumann, B., Stammler, H. - G., & Mattay, J. (2009). Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation. CRYSTENGCOMM, 11(2), 306-317.
Stoll, I., Brodbeck, R., Neumann, B., Stammler, H. - G., and Mattay, J. (2009). Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation. CRYSTENGCOMM 11, 306-317.
Stoll, I., et al., 2009. Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation. CRYSTENGCOMM, 11(2), p 306-317.
I. Stoll, et al., “Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation”, CRYSTENGCOMM, vol. 11, 2009, pp. 306-317.
Stoll, I., Brodbeck, R., Neumann, B., Stammler, H.-G., Mattay, J.: Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation. CRYSTENGCOMM. 11, 306-317 (2009).
Stoll, Ion, Brodbeck, Ralf, Neumann, Beate, Stammler, Hans-Georg, and Mattay, Jochen. “Controlling the self assembly of arene functionalised 2-aminopyrimidines by arene-perfluoroarene interaction and by silver(I) complex formation”. CRYSTENGCOMM 11.2 (2009): 306-317.
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