Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes

Gerkensmeier T, Agena C, Iwanek W, Fröhlich R, Kotila S, Nather C, Mattay J (2001)
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 56(10): 1063-1073.

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Hydroxyresorc[4]arenes are bowl-shaped calixarene compounds. Herein we report the synthesis and the results of X-ray diffraction examinations of six hydroxyresorc[4]arenes, one of them could be crystallized in two conformations. All compounds co-crystallize with different solvent molecules, linked together by hydrogen bonds. It is known that hydroxyresorc[4]arenes are capable of forming large aggregates, a number of different compounds have been prepared, some of them could be crystallized and investigated by single crystal methods. Most of the compounds tend to form polarity-induced double layers.
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Gerkensmeier T, Agena C, Iwanek W, et al. Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 2001;56(10):1063-1073.
Gerkensmeier, T., Agena, C., Iwanek, W., Fröhlich, R., Kotila, S., Nather, C., & Mattay, J. (2001). Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 56(10), 1063-1073.
Gerkensmeier, T., Agena, C., Iwanek, W., Fröhlich, R., Kotila, S., Nather, C., and Mattay, J. (2001). Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 56, 1063-1073.
Gerkensmeier, T., et al., 2001. Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 56(10), p 1063-1073.
T. Gerkensmeier, et al., “Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes”, ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, vol. 56, 2001, pp. 1063-1073.
Gerkensmeier, T., Agena, C., Iwanek, W., Fröhlich, R., Kotila, S., Nather, C., Mattay, J.: Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 56, 1063-1073 (2001).
Gerkensmeier, T, Agena, C, Iwanek, W, Fröhlich, R, Kotila, S, Nather, C, and Mattay, Jochen. “Synthesis and structural studies of 5, 11, 17, 23-tetrahydroxyresorc[4]arenes”. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 56.10 (2001): 1063-1073.
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