Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene

Mormann M, Kuck D (2002)
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS 45(7): 601-610.

Journal Article | Published | English

No fulltext has been uploaded

Author
;
Abstract
An efficient synthesis of [1-C-13]-para-xylene (1a) and [2-C-13]-para-xylene (1b) is described. The incorporation of the label has been achieved by cyclocondensation of suitable 1,5-bis(bromomagnesio)alkanes with either ethyl [1-C-13]acetate or ethyl [C-13]formate which gave [ring-C-13]-labelled dimethylcyclohexanols. Dehydration of these alcohols followed by dehydrogenation of the intermediate dimethylcyclohexenes furnished the title compounds in 32 and 40% overall yield, respectively. Copyright (C) 2002 John Wiley Sons, Ltd.
Publishing Year
ISSN
eISSN
PUB-ID

Cite this

Mormann M, Kuck D. Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS. 2002;45(7):601-610.
Mormann, M., & Kuck, D. (2002). Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 45(7), 601-610.
Mormann, M., and Kuck, D. (2002). Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS 45, 601-610.
Mormann, M., & Kuck, D., 2002. Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 45(7), p 601-610.
M. Mormann and D. Kuck, “Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene”, JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, vol. 45, 2002, pp. 601-610.
Mormann, M., Kuck, D.: Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS. 45, 601-610 (2002).
Mormann, Michael, and Kuck, Dietmar. “Synthesis of [1-C-13]-para-xylene and [2-C-13]-para-xylene”. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS 45.7 (2002): 601-610.
This data publication is cited in the following publications:
This publication cites the following data publications:

Export

0 Marked Publications

Open Data PUB

Web of Science

View record in Web of Science®

Search this title in

Google Scholar