Diaminotriazine substituted 1,3-alternate calix[4]arenes

Barton OG, Schmidtmann M, Müller A, Mattay J (2004)
NEW JOURNAL OF CHEMISTRY 28(11): 1335-1339.

Journal Article | Published | English

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Abstract
The synthesis and crystal structures of two calix[4]arenes adopting the 1,3-alternate conformation substituted at the wide rim with diaminotriazine moieties are described. The crystal structure of the disubstituted calixarene 8 is governed by the diaminotriazine moieties which form infinite bands through hydrogen bonding. Around the diaminotriazine bands the calix[4] arene backbones are placed. In contrast hydrogen bonding between the diaminotriazine moieties of the tetrasubstituted calixarene 9 favour face to face complexes resulting in infinite strands. Hydrogen bonds in both compounds 8 and 9 are broken by polar solvents as the H-1 NMR spectra in DMSO-d(6) indicates.
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Barton OG, Schmidtmann M, Müller A, Mattay J. Diaminotriazine substituted 1,3-alternate calix[4]arenes. NEW JOURNAL OF CHEMISTRY. 2004;28(11):1335-1339.
Barton, O. G., Schmidtmann, M., Müller, A., & Mattay, J. (2004). Diaminotriazine substituted 1,3-alternate calix[4]arenes. NEW JOURNAL OF CHEMISTRY, 28(11), 1335-1339.
Barton, O. G., Schmidtmann, M., Müller, A., and Mattay, J. (2004). Diaminotriazine substituted 1,3-alternate calix[4]arenes. NEW JOURNAL OF CHEMISTRY 28, 1335-1339.
Barton, O.G., et al., 2004. Diaminotriazine substituted 1,3-alternate calix[4]arenes. NEW JOURNAL OF CHEMISTRY, 28(11), p 1335-1339.
O.G. Barton, et al., “Diaminotriazine substituted 1,3-alternate calix[4]arenes”, NEW JOURNAL OF CHEMISTRY, vol. 28, 2004, pp. 1335-1339.
Barton, O.G., Schmidtmann, M., Müller, A., Mattay, J.: Diaminotriazine substituted 1,3-alternate calix[4]arenes. NEW JOURNAL OF CHEMISTRY. 28, 1335-1339 (2004).
Barton, OG, Schmidtmann, Marc, Müller, Achim, and Mattay, Jochen. “Diaminotriazine substituted 1,3-alternate calix[4]arenes”. NEW JOURNAL OF CHEMISTRY 28.11 (2004): 1335-1339.
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