A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring

Theil H, Froehlich R, Glaser T (2009)
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64(11-12): 1633-1638.

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Abstract
The Newman-Kwart rearrangement of O-thiocarbamates to S-thiocarbamates is a versatile method for the conversion of phenols into thiophenols. The triple rearrangement of the O-trithiocarbamate 2,4,6-triacetyl-1,3,5-tri-(dimethylthiocarbamoyloxy)benzene (2) to the S-trithiocarbamate 2,4,6-triacetyl-1,3,5-tri-(dimethylthiocarbamoylthio)benzene (3) is performed, which is unprecendented for fully substituted benzene rings. The synthesis and characterization of the O-trithiocarbamate 2 and the S-trithiocarbamate 3 including the single-crystal X-ray structure analysis of compound 3 are presented.
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Theil H, Froehlich R, Glaser T. A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 2009;64(11-12):1633-1638.
Theil, H., Froehlich, R., & Glaser, T. (2009). A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 64(11-12), 1633-1638.
Theil, H., Froehlich, R., and Glaser, T. (2009). A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64, 1633-1638.
Theil, H., Froehlich, R., & Glaser, T., 2009. A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 64(11-12), p 1633-1638.
H. Theil, R. Froehlich, and T. Glaser, “A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring”, ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, vol. 64, 2009, pp. 1633-1638.
Theil, H., Froehlich, R., Glaser, T.: A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 64, 1633-1638 (2009).
Theil, Hubert, Froehlich, Roland, and Glaser, Thorsten. “A Triple Newman-Kwart Rearrangement at a Fully Substituted Benzene Ring”. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64.11-12 (2009): 1633-1638.
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