An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures

Berger R, Hoffmann M, Hayes SA, Mitzel NW (2009)
ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64(11-12): 1259-1268.

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Zeitschriftenaufsatz | Veröffentlicht | Englisch
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Abstract / Bemerkung
The improvement of a Balzers Eldigraph KD-G2 gas-phase electron diffractometer, previously operated at the University of Tubingen, is reported. The diffractometer was equipped with a state-of-the-art telefocus electron gun, and high-energy radiation-sensitive imaging plates were introduced as detector system. A differential vacuum pumping system separating the diffraction chamber from the electron source was installed. A nozzle for the evaporation of compounds in a temperature range from 25 to 400 degrees C was constructed and its functionality proven by the structure determination of quinoline. Calibration, data reduction and structure refinement using standard procedures in connection with a selection of literature-known programs are described. The gas-phase structure of quinoline was determined, discussed and compared with ab initio and solid-state X-ray diffraction results.
Erscheinungsjahr
Zeitschriftentitel
ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES
Band
64
Zeitschriftennummer
11-12
Seite
1259-1268
ISSN
eISSN
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Berger R, Hoffmann M, Hayes SA, Mitzel NW. An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures. ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 2009;64(11-12):1259-1268.
Berger, R., Hoffmann, M., Hayes, S. A., & Mitzel, N. W. (2009). An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures. ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 64(11-12), 1259-1268. doi:10.1515/znb-2009-11-1204
Berger, R., Hoffmann, M., Hayes, S. A., and Mitzel, N. W. (2009). An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures. ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64, 1259-1268.
Berger, R., et al., 2009. An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures. ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 64(11-12), p 1259-1268.
R. Berger, et al., “An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures”, ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, vol. 64, 2009, pp. 1259-1268.
Berger, R., Hoffmann, M., Hayes, S.A., Mitzel, N.W.: An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures. ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES. 64, 1259-1268 (2009).
Berger, Raphael, Hoffmann, Manfred, Hayes, Stuart A., and Mitzel, Norbert W. “An Improved Gas Electron Diffractometer - The Instrument, Data Collection, Reduction and Structure Refinement Procedures”. ZEITSCHRIFT FUER NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES 64.11-12 (2009): 1259-1268.